PRODUCT DESCRIPTION. Adipic Acid. & Account Managers, For The solubility of adipic acid (1,6-hexanedioic acid) in acetone, chloroform, and toluene has been measured, respectively, at temperatures ranging from (298.15 to 323.15) K and (298.15 to 333.15) K by a static analytical method. https://doi.org/10.1016/j.molliq.2019.111735, https://doi.org/10.1016/j.jct.2019.06.033, https://doi.org/10.1016/j.molliq.2018.09.076, https://doi.org/10.1016/j.jct.2014.05.009, https://doi.org/10.1016/j.snb.2012.11.097, https://doi.org/10.1016/j.fluid.2011.01.014. It has a slight acidic taste and a very faint odor. adipic acid tableting tablet lubricant composition Prior art date 1969-07-07 Legal status (The legal status is an assumption and is not a legal conclusion. the Altmetric Attention Score and how the score is calculated. ... (25 deg C, exp database VP ) Water Solubility Estimate from Log Kow (WSKOW v1.41): Water Solubility at 25 deg C (mg/L): 1.673e+005 log Kow used: 0.08 (expkow database) no-melting pt equation used Water Sol (Exper. Current commercial adipic acid is produced from cyclohexaneby two oxidation steps. it has a ph of 2.86 at 0.6% usage level at 25°c. Mengqi Yan, Xiuqing Li, Bao Tao, Lintao Yang, Weiping Luo. It is used heavily in the production of textiles, particularly nylon. ADI 0-5 mg/kg bw, established at the 21st JECFA in 1977. Adipic Acid is an acidulant and flavoring agent. The production of nylon comes from a reaction with hexamethylene diamine, also supplied by Parchem.. Adipic acid can also be found in the production of foods as a flavoring agent to add tartness.. ADIPIC ACID Prepared at the 53rd JECFA (1999) and published in FNP 52 Add 7 (1999), superseding specifications prepared at the 19th JECFA (1975), published in NMRS 55B (1976) and in FNP 52 (1992). Fátima L. Mota, António J. Queimada, Simão P. Pinho, Eugénia A. Macedo. You have to login with your ACS ID befor you can login with your Mendeley account. always use the smallest container you can to make measurements and to do experiments. The solubility of adipic acid in methanol, ethanol, propanol, isopropanol, n-butanol, tert-butanol, acetone, 1,4-dioxane, acetic acid, and water was measured within the 0–60°C temperature range. TECHNICAL DATA. FIRST-AID MEASURES Eyes Rinse with plenty of water for at least 15 minutes and seek medical attention immediately. b. it is used in powdered drinks, beverages, gelatin desserts, loz- … it is characterized as stable, nonhygroscopic, and slightly soluble, with a water solubility of 1.9 g/100 ml at 20°c. The C6 straight-chain dicarboxylic acid is slightly soluble in water and soluble in alcohol and acetone. The substance is a weak acid. Weiping Luo, Xiuqing Li, Dong Ruan, Dawei Liu, Kaili Xie, Jing Wang, Wei Deng, Qiang Liu, and Zhaoke Chen . Adipic Acid occurs as white crystals or a crystalline powder. A modified Apelblat equation was used to correlate the experimental data. CAS: 124-04-9. It is freely soluble in alcohol, soluble in acetone, and slightly soluble in water. The Effect of Temperature on the Solubility of 11-Cyanoundecanoic Acid in Cyclohexane, n-Hexane, and Water. Sile Shi, Mengqi Yan, Bao Tao, Weiping Luo. 1. Adipic acid or hexanedioic acid is the organic compound with the formula (CH2)4(COOH)2. 18 publications. Adipic acid is a white crystalline solid. Adipic acid is also used in baking powders instead of cream of tartar and other foods. solubilities. What is the Kd of adipic acid. Get medical attention. A sampler for determination of the temperature dependence of the solubility of solids in liquids by the isothermal method was suggested. Expired - Lifetime Application number Inventor George Carr Hoss It is a precursor to diverse industrial products that include polymers, plasticizers, and as a component of many hair and skin conditioners. 3 decimal place balance. Marcus A. O’Mahony, Denise M. Croker, Åke C. Rasmuson, Stéphane Veesler, and Benjamin K. Hodnett . APPEARANCE. USE: Adipic acid is a commercially important chemical used during the production of nylon, plastics, lubricants, adhesives, and polyurethane foam. RHODIACID AA - ADIPIC ACID Revision Date 28.02.2020 PRCO90076334 Version : 3.00 / GB ( EN ) 1 / 37 SECTION 1: Identification of the substance/mixture and of the company/undertaking 1.1 Product identifier - Trade name RHODIACID AA - ADIPIC ACID - Index-No. 355 DEFINITION Chemical names Hexanedioic acid, 1,4-Butanedicarboxylic acid Determination and Correlation of Solubilities for Succinic Acid in the Adipic Acid + Glutaric Acid + Acetone Mixture and Adipic Acid in the Succinic Acid + Glutaric Acid + Acetone Mixture. If breathing is difficult, give oxygen. Adipic acid (AA) CAS-No 124-04-9 . of applications: resins, adhesives, coatings, plastics, paper, plasticizers, detergency . Adipic Acid TCC’s Adipic Acid is a mildly toxic, white, crystalline compound. Ximeng Yu, Zhongquan Shen, Qing Sun, Nianlong Qian, Chao Zhou, and Jizhong Chen . White crystalline powder. Conventionally it was manufactured from petrochemicals but in recent days it can be synthesized from renewable substrates by means of biological methods. Solubilities of Adipic Acid and Succinic Acid in a Glutaric Acid + Acetone or n-Butanol Mixture. Also, it is less soluble in water and is soluble in alcohol and acetone. The key difference between adipic acid and salicylic acid is that adipic acid contains two carboxyl acid groups, whereas salicylic acid contains one carboxyl acid group per molecule.. Adipic acid and salicylic acid are organic compounds. An 84% conversion of adipic acid's carbon content to carbon dioxide was observed after 30 days aerobic incubation in soil biometer flasks at 151-152 °C (for adipic acid) EU Food Improvement Agents 3.2.3 Solubility Approximately 50 g/100 ml water (20 °C) Adipic acid is an aliphatic dicarboxylic acid with the formula (CH2)4 (COOH)2. Yanyan Li, Yatao Wang, Zhuoyuan Ning, Jianfang Cui, Qiaoye Wu, and Xunqiu Wang . 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The solubility of adipic acid in methanol, ethanol, propanol, isopropanol, n -butanol, tert -butanol, acetone, 1,4-dioxane, acetic acid, and water was measured within the 0–60°C temperature range. Your Mendeley pairing has expired. This produces toxic and corrosive fumes of valeric acid and other substances. Sign in to download full-size image Figure 27. Andreia de P.M. da Silva, Priscilla B. de Oliveira, Thiago B. Bandini, Amaro G. Barreto Junior, Rodrigo C. de Sena, João F. Cajaiba da Silva. Weiping Luo, Mengqi Yan, Bao Tao, Sile Shi, Bo Chen. Other patented processes include those using phenolas feedst… Adipic acid is present in some plants and is a chemical in tobacco and tobacco smoke. Low-cost system based on image analysis to determine solubility curves. Adipic Acid. Semantic Scholar is a free, AI-powered research tool for scientific literature, based at the Allen Institute for AI. The solubility of adipic acid in cyclohexanol and cyclohexanone is lower than that in acetic acid. Inhalation Move casualty to fresh air and keep at rest. Mobility. It is very soluble in water. This probably attributes to the incompatible structures. Determination of the Adipic Acid Solubility Curve in Acetone by Using ATR-FTIR and Heat Flow Calorimetry. The different solubility of adipic acid in various solvents results mainly from the structure and solvent polarity. It is insoluble in water. Immediate steps should be taken to limit its spread to the environment. DOI: 10.1016/j.molliq.2018.09.076. Find more information about Crossref citation counts. Historically, adipic acid was prepared from various fats using oxidation. These metrics are regularly updated to reflect usage leading up to the last few days. Measurement and Correlation for Solubilities of Adipic Acid, Glutaric Acid and Succinic Acid in Acetic Acid + Cyclohexanone Mixtures. Get article recommendations from ACS based on references in your Mendeley library. Cyclohexane + O2 → cyclohexanol and cyclohexanone 2. cyclohexanol/cyclohexanone + nitric acid+ air → adipic acid + nitrous oxide (The mixture of cyclohexanol and cyclohexanone produced from cyclohexane is commercially called "KA oil", the abbreviation of "Ketone-Alcohol oil".) Industrial & Engineering Chemistry Research. Formula: C 6 H 1 0 O 4 / HOOC(CH 2) 4 COOH Molecular mass: 146.14 Boiling point: 338°C Melting point: 152°C Density: 1.36 g/cm³ Solubility in water, g/100ml at 15°C: 1.4 (moderate) Weiping Luo, Dong Ruan, Dawei Liu, Kaili Xie, Xiuqing Li, Wei Deng, and Cancheng Guo . It is a white, crystalline compound with a slight acid taste and very faint odor. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.) Citations are the number of other articles citing this article, calculated by Crossref and updated daily. A sampler for determination of the temperature dependence of the solubility of solids in liquids by the isothermal method was suggested. It is an emulsifier for Drilling Muds and Fluids as well. Adipic acid is found to be associated with HMG-CoA lyase deficiency, carnitine-acylcarnitine translocase deficiency, malonyl-Coa decarboxylase deficiency, and medium Chain acyl-CoA dehydrogenase deficiency, which are inborn errors of metabolism. An odd–even effect on solubility of dicarboxylic acids in organic solvents. From an industrial perspective, it is the most important dicarboxylic acid: about 2.5 billion kilograms of this white crystalline powder are produced annually, mainly as a precursor for the production of nylon. Environmental: Adipic acid is not expected to volatilize from dry soil surfaces based on its extrapolated vapor pressure. Solubility of succinic acid, glutaric acid and adipic acid in propionic acid + ε-caprolactone + water mixtures: Experimental measurement and thermodynamic modeling. Reviewers, Librarians It is mainly as a precursor for the production of nylon. Biodegradability screening tests indicate that adipic acid is readily biodegradable. Dongwei Wei, Hui Li, Cheng Liu, and Baohe Wang . Journal of Molecular Liquids 2018, 272, 106-119. Measurement and correlation for solubilities of succinic acid, glutaric acid and adipic acid in five organic solvents. You are currently offline. The solubility of adipic acid in methanol, ethanol, propanol, isopropanol, n-butanol, tert-butanol, acetone, 1,4-dioxane, acetic acid, and water was measured within the 0–60°C temperature range. Its solubility is very low in water and soluble in organic solvents like alcohol and acetone. Adipic Acid also known as Hexane-1,6-dioic acid is a dibasic acid with the molecular formula C 3 H 8 O 4, CAS 124-04-9.Adipic acid is slightly soluble in water and soluble in alcohol and acetone. The dependence of the solubility on the solvent and temperature was…, Solubility of Adipic Acid in Acetone, Chloroform, and Toluene, Investigation on solubility of hydroxy dibasic acids in alkanolamine solutions, Solubilities of Adipic Acid and Succinic Acid in a Glutaric Acid + Acetone or n-Butanol Mixture, Determination of the Adipic Acid Solubility Curve in Acetone by Using ATR-FTIR and Heat Flow Calorimetry, Solubility and thermodynamics of vitamin C in binary liquid mixtures involving water, methanol, ethanol and isopropanol at different temperatures, Thermodynamics of cis,cis-muconic acid solubility in various polar solvents at low temperature range, Measurement and Correlation of the Solubility for 4,4′-Diaminodiphenylmethane in Different Solvents, KINETICS AND MECHANISM OF OXIDATION OF MIXTURE OF OXALIC ACID AND ADIPIC ACID BY CHROMIC ACID IN PRESENCE OF ACETIC ACID, Measurement and Correlation for Solubilities of Adipic Acid, Glutaric Acid, and Succinic Acid in Dimethyl Adipate + Methanol Mixtures, Measurement and Correlation for Solubilities of Adipic Acid, Glutaric Acid and Succinic Acid in Acetic Acid + Cyclohexanone Mixtures, The solubilities of dicarboxylic acids in benzene and aqueous solutions, By clicking accept or continuing to use the site, you agree to the terms outlined in our. A Unified Thermodynamics Model for Solid–Liquid Equilibrium, Liquid–Liquid Equilibrium, and Vapor–Liquid Equilibrium of Cyclohexane Oxidation Systems: NRTL Model. The solubility of adipic acid (1,6-hexanedioic acid) in acetone, chloroform, and toluene has been measured, respectively, at temperatures ranging from (298.15 to 323.15) K and (298.15 to 333.15) K by a static analytical method. adipic acid and solubility-very soluble in hot water and almost insoluble in cold water-so water is an ideal solvent for recrystallization of this compound. Function: Buffer; neutralizing agent. Adipic acid is a straight-chain aliphatic dicarboxylic acid, commonly used in the manufacturing of nylon-6,6 and plasticizers. Please note: If you switch to a different device, you may be asked to login again with only your ACS ID. Hui Zhang, Qiuxiang Yin, Zengkun Liu, Junbo Gong, Ying Bao, Meijing Zhang, Hongxun Hao, Baohong Hou, Chuang Xie. It is not hygroscopic. It is slightly soluble in water and soluble in alcohol and acetone. A sampler for determination of the temperature dependence of the solubility of solids in liquids by the isothermal method was suggested. Decomposes on heating. CAS Number: 124-04-9 Formula Weight: 146.14 Formula: HO 2 C(CH 2 ) 4 CO 2 H Density (g/mL): 1.34 Boiling Point (°C): 377 Freezing Point (°C): 152 Solubility: Acetone and Alcohol Synonyms: Hexanedioic Acid Shelf Life (months): 12 Storage: GreenChemicals for science education are available in easy-to-use formats with instructions for students to be introduced to a variety of subjects. SYNONYMS INS No. The compositions of the adipic acid in saturated solution were analyzed by acid−base titration. The non-toxic saturated dicarboxylic acid is produced as a white powder. Find more information about Crossref citation counts. Article Views are the COUNTER-compliant sum of full text article downloads since November 2008 (both PDF and HTML) across all institutions and individuals. 607-144-00-9 - REACH : Registration number 01-2119457561-38-0009 Clicking on the donut icon will load a page at altmetric.com with additional details about the score and the social media presence for the given article. The Altmetric Attention Score is a quantitative measure of the attention that a research article has received online. a. This carboxylic acid is vital to industry. COMPOSITION. Adipic acid otherwise rarely occurs in nature, but it is known as manufactured E number food additive E355. Solubility of succinic acid, glutaric acid and adipic acid in propionic acid + ε-caprolactone mixtures and propionic acid + cyclohexanone mixtures: Experimental measurement and thermodynamic modeling. Solubility prediction, solvate and cocrystal screening as tools for rational crystal engineering. Adipic acid is used as precursor in manufacture of nylon. Solubilities of Adipic Acid in Cyclohexanol + Cyclohexanone Mixtures and Cyclohexanone + Cyclohexane Mixtures. Adipic Acid Chemical Structure Composition. Andreia de P. M. da Silva and João F. Cajaiba da Silva . Will likely be mobile in the environment due to its water solubility. The primary hazard is the threat to the environment. Please reconnect, Authors & Fei Wang, Yanyan Li, Zhuoyuan Ning, Chunhua Jiang, and Xunqiu Wang . expressed as [adipic acid]water/[adipic acid]ether? use 3 decimal places. Adipic acid EC50= 31.3 mg/L 72h EC50 = 26.6 mg/L 96h Leuciscus idus: LC50 = 230 mg/L 96h EC50 = 91.9 mg/L 17 hEC50 = 85.7 mg/L 48h Persistence and DegradabilityPersistence is unlikely Bioaccumulation/ AccumulationNo information available. Calculate the fraction of adipic acid that. Microscale Solubility Measurements of Matrix-Assisted Laser Desorption–Ionization (MALDI) Matrices Using Attenuated Total Reflection (ATR) Fourier Transform Infrared Spectroscopy (FT-IR) Coupled with Partial Least Squares (PLS) Analysis. Solubility of succinic acid, glutaric acid and adipic acid in propionic acid + ε-caprolactone mixtures and propionic acid + cyclohexanone mixtures: Experimental measurement and thermodynamic modeling. The compositions of the adipic acid in saturated solution were analyzed by acid−base titration. Adipic Acid × × Purity: >99.0%(GC ... Solubility in Methanol: almost transparency: Properties (reference) Melting Point: 153 °C: Solubility in water: Slightly soluble: Degree of solubility in water : 22 g/l 20 °C: Solubility (very soluble in) Alcohol: Solubility (soluble in) Solubilities of Adipic Acid, Glutaric Acid, and Succinic Acid in Dimethyl Glutarate + Methanol Mixtures: Experimental Measurement and Thermodynamic Modeling. Bo Chen, Mengqi Yan, Bao Tao, Lintao Yang. Some features of the site may not work correctly. This organic compound is the most important synthetic dicarboxylic acid produced annually. The thermodynamic parameters of solution of adipic acid in the above solvents were calculated. Measurement and Correlation for Solubilities of Adipic Acid in Acetic Acid + ε-Caprolactone Mixtures and Cyclohexanone + ε-Caprolactone Mixtures. The solubility of adipic acid in water is 1.5 g. per 100 mL at 15?C, and 0.6 g per 100 mL in. Reacts with oxidizing materials. High purity Adipic Acid used for the production of nylon 66 and for a wide range . Remember the Kd is usually the ratio of. Adipic Acid >99 124-04-9 204-673-3 C 6 H 10 O 4 146.14 g/mol 4. Adipic acid [ACD/IUPAC Name] [Wiki] Adipinsäure [German] [ACD/IUPAC Name] Asapic. If not breathing, give artificial respiration. Librarians & Account Managers. Adipic acid (butane-1,4-dicarboxylic acid, C6 H 10 O 4) (Figure 27) is a white crystalline powder of C6-straight chain dicarboxylic acid, and is one of the most used chemicals in the world today (Table 1). Nearly all commercial adipic acid is produced from cyclohexane. You’ve supercharged your research process with ACS and Mendeley! Azelaic acid is an organic compound found in wheat, rye, and barley. ether at the same temperature. Weiping Luo, Mengqi Yan, XiaoXiao Sheng, Bao Tao, Sile Shi, Wei Deng, Weijun Yang. Measuring the Solubility of a Quickly Transforming Metastable Polymorph of Carbamazepine. Solubility of drug-like molecules in pure organic solvents with the CPA EoS. They contain carboxylic groups as their functional group.However, they have different chemical and physical properties as well as different applications. Find more information on the Altmetric Attention Score and how the score is calculated. Malonic acid (IUPAC systematic name: propanedioic acid) is a dicarboxylic acid with structure CH 2 (COOH) 2.The ionized form of malonic acid, as well as its esters and salts, are known as malonates.For example, diethyl malonate is malonic acid's diethyl ester.The name originates from the Greek word μᾶλον (malon) meaning 'apple'. Solubility of Adipic Acid in Acetone, Chloroform, and Toluene, Research and Development Center for Petrochemical Technology, Tianjin University, Tianjin 300072, P. R. China. Model for Solid–Liquid Equilibrium, Liquid–Liquid Equilibrium, and Xunqiu Wang: //doi.org/10.1016/j.molliq.2018.09.076, https: //doi.org/10.1016/j.snb.2012.11.097, https //doi.org/10.1016/j.snb.2012.11.097. Valeric acid and Succinic acid in saturated solution were analyzed by acid−base titration acetone by using ATR-FTIR and Heat Calorimetry... Compound with the formula ( CH2 ) 4 ( COOH ) 2 Mixtures and Cyclohexanone + Cyclohexane Mixtures in.... 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